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Type: Journal article
Title: Synthesis of per-deuterated alkyl amines for the preparation of deuterated organic pyromellitamide gelators
Author: Yepuri, N.
Jamieson, S.
Darwish, T.
Rawal, A.
Hook, J.
Thordarson, P.
Holden, P.
James, M.
Citation: Tetrahedron Letters: the international journal for the rapid publication of all preliminary communications in organic chemistry, 2013; 54(20):2538-2541
Publisher: Elsevier
Issue Date: 2013
ISSN: 0040-4039
Statement of
Nageshwar R.Yepuri, Scott A.Jamieson, Tamim A.Darwish, Aditya Rawal, James M.Hook ... Michael James ... et al.
Abstract: A general, direct and scalable synthesis of per-deuterated alkyl amines is reported, together with their incorporation into pyromellitamides, which form self-assembled gels in cyclohexane. The deuterium labelling of these gelators allows the study of the dynamic intermolecular interactions in these materials using solid-state 2H NMR spectroscopy.
Keywords: Self-assembling organogels; deuterated amines; supramolecular chemistry; solid state deuterium NMR
Rights: © 2013 Published by Elsevier Ltd. All rights reserved.
DOI: 10.1016/j.tetlet.2013.03.031
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