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Type: Journal article
Title: Synthesis of macrocyclic β-Strand memplates by ring closing metathesis
Other Titles: Synthesis of macrocyclic beta-Strand memplates by ring closing metathesis
Author: Abell, A.
Alexander, N.
Aitken, S.
Chen, H.
Coxon, J.
Jones, M.
McNabb, S.
Muscroft-Taylor, A.
Citation: Journal of Organic Chemistry, 2009; 74(11):4354-4356
Publisher: Amer Chemical Soc
Issue Date: 2009
ISSN: 0022-3263
Statement of
Andrew D. Abell, Nathan A. Alexander, Steven G. Aitken, Hongyuan Chen, James M. Coxon, Matthew A. Jones, Stephen B. McNabb and Andrew Muscroft-Taylor
Abstract: We report the synthesis of macrocycles 1-6 via ring closing metathesis of dienes 7-12. Addition of chlorodicyclohexylborane to thermal and microwave assisted RCM of dienes 8 and 9 markedly improves the yield. The geometric isomers of macrocycles 1-3 and 5 have been assigned using X-ray crystallography and NMR.
Rights: © 2009 American Chemical Society
RMID: 0020091402
DOI: 10.1021/jo802723w
Appears in Collections:Chemistry publications

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