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Type: Journal article
Title: 5-Bromospiro[1,2-dioxane-4,4'-tricyclo[,8]undecane]-3'-ol
Author: Robinson, A.
Taylor, D.
Tiekink, E.
Citation: Acta Crystallographica Section E: Structure Reports Online, 2010; 66(1):O247-U3231
Publisher: Blackwell Munksgaard
Issue Date: 2010
ISSN: 1600-5368
Statement of
T. V. Robinson, D. K. Taylor and E. R. T. Tiekink
Abstract: The title compound, C14H21BrO3, comprises a seven- (C7) and three six-membered (1 × O2C4 and 2 × C6) rings, and each adopts a conformation based on a chair. Stability to the molecular structure is afforded by an intramolecular O-HBr hydrogen bond. In the crystal structure, molecules are arranged into a helical supramolecular chain along the b axis, linked by C-HO interactions, where the O-atom acceptor is one of the dioxane O atoms. The crystal studied was found to be a racemic twin. The major component was present 94% of the time.
Rights: Copyright © 2010 International Union of Crystallography
DOI: 10.1107/S1600536809054762
Grant ID: ARC
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