Innovative self-healing composites using steel slag and chitosan

Date

2024

Authors

Liu, Y.
Zhuge, Y.
Duan, W.
Sanaei Ataabadi, H.
Jia, Q.
Zeng, J.
Yoo, D.Y.

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Journal article

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Cement and Concrete Composites, 2024; 152

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Abstract

An innovative capsule using steel slag as the primary core material complemented by chitosan as a secondary core material was developed. Steel slag exhibited virtually no hydraulic reactivity but readily underwent carbonation. The designed capsule was proven to help enhance the self-healing capabilities of cement-based composites at CO₂ concentrations of 3 %. This approach not only offers a cost-effective solution for artificial capsules but also proposes the possibility of using high CO₂ environments (e.g., sewage) as natural carbonation chambers. Mineralogy analysis of steel slag, sourced from the Australian local industry, identified a composition primarily consisting of larnite, srebrodolskite, and RO phases. Larnite exhibits considerable reactivity to carbonation. The carbonation mechanism of steel slag at 3 % CO₂ concentration was investigated. The addition of a minor content of chitosan can significantly improve the carbonation level of steel slag by promoting the dissolution of calcium ions. After 28 days of healing, the CO₂ uptake of the slag mixed with chitosan reaches 4.6 %, resulting in the formation of 6.0 % by weight of CaCO₃ in the paste. Such a carbonation level was sufficient to efficiently heal cracks and improve the self-healing performance of cement-based composites. Most cracks below 200 μm were highly possible to be closed at 28 days of carbonation healing. The main healing products consisted of cubic-shaped CaCO₃ and C-(A)-S-H gel, deriving from the carbonation of steel slag and the pozzolanic reaction of silica gel after calcium leaching, respectively.

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Data source: Supplementary data, https://doi.org/10.1016/j.cemconcomp.2024.105652

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Copyright 2024 The Author(s). Published by Elsevier Ltd. This is an open access article under the CC BY license (https://creativecommons.org/licenses/by/4.0/)

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