Ammonia electrosynthesis with high selectivity under ambient conditions via a Li+ incorporation strategy

Date

2017

Authors

Chen, G.-F.
Cao, X.
Wu, S.
Zeng, X.
Ding, L.-X.
Zhu, M.
Wang, H.

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Journal article

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Journal of the American Chemical Society, 2017; 139(29):9771-9774

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Gao-Feng Chen, Xinrui Cao, Shunqing Wu, Xingye Zeng, Liang-Xin Ding, Min Zhu and Haihui Wang

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Abstract

We report the discovery of a dramatically enhanced N2 electroreduction reaction (NRR) selectivity under ambient conditions via the Li+ incorporation into poly(N-ethyl-benzene-1,2,4,5-tetracarboxylic diimide) (PEBCD) as a catalyst. The detailed electrochemical evaluation and density functional theory calculations showed that Li+ association with the O atoms in the PEBCD matrix can retard the HER process and can facilitate the adsorption of N2 to afford a high potential scope for the NRR process to proceed in the "[O-Li+]·N2-Hx" alternating hydrogenation mode. This atomic-scale incorporation strategy provides new insight into the rational design of NRR catalysts with higher selectivity.

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© 2017 American Chemical Society

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