Nucleophilic properties of Ru(C CH)(dppe)Cp*: Synthesis and structure of Ru{c-C=CArC(O)C(O)O}(dppe)Cp* [Ar=2,4-(NO2)2C6H3]
Date
2011
Authors
Bruce, M.
Morris, J.
Parker, C.
Skelton, B.
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Journal of Organometallic Chemistry, 2011; 696(21):3292-3295
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Michael I. Bruce, Jonathan C. Morris, Christian R. Parker and Brian W. Skelton
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Abstract
The complex Ru{c-CCArC(O)C(O)O}(dppe)Cp* [Ar = 2,4-(NO <inf>2</inf>)<inf>2</inf>C<inf>6</inf>H<inf>3</inf>] 2, containing a dihydrofuran-3,4-dione ligand, was obtained from a reaction between the strong nucleophile Ru(CCH)(dppe)Cp* 1 and bis(2,4-dinitrophenyl) oxalate. The X-ray determined molecular structure of 2 is reported, together with a plausible route for its formation. © 2011 Elsevier B.V. All rights reserved.
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© 2011 Elsevier B.V. All rights reserved.