Pentavalent Uranium Incorporated in the Structure of Proterozoic Hematite.

Date

2022

Authors

Ilton, E.S.
Collins, R.N.
Ciobanu, C.L.
Cook, N.J.
Verdugo-Ihl, M.
Slattery, A.D.
Paterson, D.J.
Mergelsberg, S.T.
Bylaska, E.J.
Ehrig, K.

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Environmental Science and Technology, 2022; 56(16):11857-11864

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Eugene S. Ilton, Richard N. Collins, Cristiana L. Ciobanu, Nigel J. Cook, Max Verdugo-Ihl, Ashley D. Slattery, David J. Paterson, Sebastian T. Mergelsberg, Eric J. Bylaska, and Kathy Ehrig

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Abstract

Characterizing the chemical state and physical disposition of uranium that has persisted over geologic time scales is key for modeling the longterm geologic sequestration of nuclear waste, accurate uranium−lead dating, and the use of uranium isotopes as paleo redox proxies. X-ray absorption spectroscopy coupled with molecular dynamics modeling demonstrated that pentavalent uranium is incorporated in the structure of 1.6 billion year old hematite (α- Fe2O3), attesting to the robustness of Fe oxides as waste forms and revealing the reason for the great success in using hematite for petrogenic dating. The extreme antiquity of this specimen suggests that the pentavalent state of uranium, considered a transient, is stable when incorporated into hematite, a ubiquitous phase that spans the crustal continuum. Thus, it would appear overly simplistic to assume that only the tetravalent and hexavalent states are relevant when interpreting the uranium isotopic record from ancient crust and contained ore systems.

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© 2022 American Chemical Society

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