Soft-templating synthesis of N-Doped mesoporous carbon nanospheres for enhanced oxygen reduction reaction

Date

2015

Authors

Bayatsarmadi, B.
Zheng, Y.
Jaroniec, M.
Qiao, S.

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Journal article

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Chemistry - An Asian Journal, 2015; 10(7):1546-1553

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Bita Bayatsarmadi, YaoZheng, Mietek Jaroniec and Shi Zhang Qiao

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Abstract

The development of ordered mesoporous carbon materials with controllable structures and improved physicochemical properties by doping heteroatoms such as nitrogen into the carbon framework has attracted a lot of attention, especially in relation to energy storage and conversion. Herein, a series of nitrogen-doped mesoporous carbon spheres (NMCs) was synthesized via a facile dual soft-templating procedure by tuning the nitrogen content and carbonization temperature. Various physical and (electro)chemical properties of the NMCs have been comprehensively investigated to pave the way for a feasible design of nitrogen-containing porous carbon materials. The optimized sample showed a favorable electrocatalytic activity as evidenced by a high kinetic current and positive onset potential for oxygen reduction reaction (ORR) due to its large surface area, high pore volume, good conductivity, and high nitrogen content, which make it a highly efficient ORR metal-free catalyst in alkaline solutions.

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© 2015 Wiley-VCH Verlag GmbH &Co. KGaA, Weinheim

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