MXene Analogue: A 2D Nitridene Solid Solution for High Rate Hydrogen Production

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2022

Authors

Jin, H.
Yu, H.
Li, H.
Davey, K.
Song, T.
Paik, U.
Qiao, S.

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Angewandte Chemie International Edition, 2022; 61(27)

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Dr. Huanyu Jin, Dr. Huimin Yu, Dr. Haobo Li, Prof. Kenneth Davey, Dr. Taeseup Song, Prof. Ungyu Paik, Prof. Shi-Zhang Qiao

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Abstract

Electrocatalysts for high-rate hydrogen evolution reaction (HER) are crucial to clean fuel production. Nitrogen-rich 2D transition metal nitride, designated “nitridene”, has shown promising HER performance because of its unique physical/chemical properties. However, its synthesis is hindered by the sluggish growth kinetics. Here for the first time using a catalytic molten-salt method, we facilely synthesized a V−Mo bimetallic nitridene solid solution, V0.2Mo0.8N1.2, with tunable electrocatalytic property. The molten-salt synthesis reduces the growth barrier of V0.2Mo0.8N1.2 and facilitates V dissolution via a monomer assembly, as confirmed by synchrotron spectroscopy and ex situ electron microscopy. Furthermore, by merging computational simulations, we confirm that the V doping leads to an optimized electronic structure for fast protons coupling to produce hydrogen. These findings offer a quantitative engineering strategy for developing analogues of MXenes for clean energy conversions.

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First published: 19 April 2022

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© 2022 The Authors.Angewandte Chemie International Edition published by Wiley-VCHGmbH.This is an open access article under the terms of the Creative Commons Attribution License,which permits use, distribution and reproduction in any medium,provided the original work is properly cited.

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