Asymmetric synthesis of cyclo-archaeol and β-glucosyl cyclo-archaeol

Date

2013

Authors

Ferrer, C.
Fodran, P.
Barroso, S.
Gibson, R.
Hopmans, E.
Damsté, J.
Schouten, S.
Minnaard, A.

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Organic and Biomolecular Chemistry, 2013; 11(15):2482-2492

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Catalina Ferrer, Peter Fodran, Santiago Barroso, Robert Gibson, Ellen C. Hopmans, Jaap Sinninghe Damsté, Stefan Schouten and Adriaan J. Minnaard

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Abstract

An efficient asymmetric synthesis of cyclo-archaeol and β-glucosyl cyclo-archaeol is presented employing catalytic asymmetric conjugate addition and catalytic epoxide ring opening as the key steps. Their occurrence in deep sea hydrothermal vents has been confirmed by chromatographic comparison with natural samples.

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This journal is © The Royal Society of Chemistry 2013

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