Conversion of organic halides to disulfanes using KCN and CS₂
Date
2017
Authors
Abbasi, M.
Nowrouzi, N.
Borazjani, S.G.
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Journal article
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Tetrahedron Letters: the international journal for the rapid publication of all preliminary communications in organic chemistry, 2017; 58(45):4251-4254
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Mohammad Abbasi, Najmeh Nowrouzi, Saeedeh Ghassab Borazjani
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Abstract
A sulfur transfer reagent was produced in situ upon stirring a mixture of KCN and CS2 in DMF at r.t. for 15 min, which after heating with an alkyl halide or aryl halide and CuI gave the corresponding symmetric dialkyl or diaryl disulfide, respectively, in high to excellent yields.
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© 2017 Elsevier Ltd. All rights reserved.