Strong Electronic Interactions of the Abundant Cu/Ce Interfaces Stabilized Cu₂O for Efficient CO₂ Electroreduction to C₂₊ Products under Large Current Density

Date

2025

Authors

Li, Y.
Zou, J.
Sun, L.
Liu, S.
Li, H.
Song, Z.
Yu, J.
Zhang, L.
Guo, Z.

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Journal article

Citation

Advanced Functional Materials, 2025; 35(46):2509899-1-2509899-8

Statement of Responsibility

Yuanrui Li, Jinshuo Zou, Lidan Sun, Siqi Liu, Huiqi Li, Zhongxin Song, Jun Yu, Lei Zhang, Zaiping Guo

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Abstract

Copper-based nanocatalysts, represented by Cu₂O nanocubes, are crucial for electrocatalytic CO₂ conversion to C₂₊ products but face significant stability challenges. Structural reconstruction from Cu dissolution and reduction under negative potentials undermines their long-term stability. Herein, a novel Cu₂O@CeOₓ core-shell nanocatalyst is introduced, featuring a Cu₂O nanocube core encapsulated by an amorphous CeOₓ shell. Due to the facilitated electron transfer of abundant Cu/Ce interfaces, the CeOₓ shell layer simultaneously prevents the agglomeration and maintains the oxidation state of Cu₂O nanocubes, bringing in significantly improved stability. Unlike conventional coating layers, the defective CeOₓ shell uniquely avoids obstructing mass transfer while effectively promoting the activation of CO₂ and optimizing the electronic structure of Cu. The Cu₂O@CeOₓ nanocatalyst delivers a remarkable C₂₊ Faradaic efficiency exceeding 80% at 300 mA cm¯² under a low applied potential of −0.98 V, with exceptional durability lasting over 50 h, compared to just 2 h for Cu₂O alone. This work presents an effective strategy to enhance catalyst stability without sacrificing activity, advancing the design of durable catalysts for electrocatalytic applications.

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First published: 30 May 2025

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© 2025 Wiley-VCH GmbH.

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