Catalytic transformation of microplastics to functional carbon for catalytic peroxymonosulfate activation: Conversion mechanism and defect of scavenging

Date

2024

Authors

Ren, S.
Xu, X.
Zhu, Z.S.
Yang, Y.
Tian, W.
Hu, K.
Zhong, S.
Yi, J.
Duan, X.
Wang, S.

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Applied Catalysis B: Environmental, 2024; 342:123410-1-123410-11

Statement of Responsibility

Shiying Ren, Xin Xu, Zhong-Shuai Zhu, Yangyang Yang, Wenjie Tian, Kunsheng Hu, Shuang Zhong, Jiabao Yi, Xiaoguang Duan, Shaobin Wang

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Abstract

Plastic wastes were catalytically transformed into different structured carbons as effective catalysts for peroxymonosulfate activation to degrade organic pollutants in water and the catalytic conversion mechanism was comprehensively investigated. A salt template-based carbonization approach was successfully developed to catalytically converting high-density polyethylene (HDPE) into diverse carbon materials, such as core-shell carbon composites, nanosheets, and their hybrids. The morphology and proportions of structure defective carbon were found to be controlled by a NiCl2 to HDPE ratio. Carbon nanosheets performed excellent catalytic efficiency in peroxymonosulfate activation toward phenol oxidation, due to a high content of reactive defects via a nonradical electron-transfer mechanism. More importantly, deliberate experiment design and kinetic analyses were employed to illustrate the artifact of radical scavengers (e.g., ethanol) in mechanistic investigation for nonradical/radical reaction. This work provides an upcycle approach for waste plastics into carbocatalysts and new insight to the conversion process and advanced water purification.

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© 2023 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).

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