Total synthesis of variolin B

Date

2001

Authors

Anderson, Regan James
Morris, Jonathan Charles

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Tetrahedron Letters, 2001; 42(49):8697-8699

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Regan J. Anderson and Jonathan C. Morris

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Abstract

The total synthesis of the marine alkaloid variolin B has been achieved in eight steps, starting from commercially available 4-chloro-2-methylthiopyrimidine. The key reaction involves the tandem deoxygenation and cyclization of a triarylmethanol using a combination of triethylsilane and trifluoroacetic acid.

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School of Chemistry and Physics : Chemistry

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